analitica ph metrie mediu hidru

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TIRTRARE pH-metrica a ioniilor metalici in unui exces de EDTA,cu solutie Calcul concentratie: Cn Mn+= Cn NAOH x FNaOH x (Vs NaOH/ Vs Mn+) Titrare: Nr Vs NaOH (pH V' (ml) d1pH/dV V" (ml) d2pH/V' 1 0 2.24 0.50 0.1 1.00 4.44E-16 2 1 2.34 1.50 0.1 2.00 0.1 3 2 2.44 2.50 0.2 3.00 0.02 4 3 2.64 3.50 0.22 4.00 -0.05 5 4 2.86 4.50 0.17 5.00 0.1 6 5 3.03 5.50 0.27 6.00 0.24 7 6 3.3 6.50 0.51 7.00 1.97 8 7 3.81 7.50 2.48 8.00 1.51 9 8 6.29 8.50 3.99 9.00 -3.67 10 9 10.28 9.50 0.32 10.00 -0.12 11 10 10.6 10.50 0.2 11.00 -0.08 12 11 10.8 11.50 0.12 12.00 -0.01 13 12 10.92 12.50 0.11 13.00 -0.03 14 13 11.03 13.50 0.08 14.00 -0.01 15 14 11.11 14.50 0.07 15.00 -0.01 16 15 11.18 15.50 0.06 16.00 -0.03 17 16 11.24 16.50 0.03 17.00 0.03 18 17 11.27 17.50 0.06 18.00 -0.01 19 18 11.33 18.50 0.05 19.00 -0.02 20 19 11.38 19.50 0.03 20.00 0.02 21 20 11.41 20.50 0.05 21.00 -0.02 22 21 11.46 21.50 0.03 22.00 -0.01 23 22 11.49 22.50 0.02 23.00 0.01 24 23 11.51 23.50 0.03 23.75 0.901667 25 24 11.54 24.00 0.480833 24.00 0.020035 Masa=0,0997,la equivalent pH=6,8 Eg: 1000*0,0997/(0,1*1*7,3) 136.5753 -10 -5 0 5 10 15 20 25 30

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Sheet1TIRTRARE pH-metrica a ioniilor metalici in unui exces de EDTA,cu solutie standard de NaOHCalcul concentratie:Cn Mn+= Cn NAOH x FNaOH x (Vs NaOH/ Vs Mn+)Titrare:NrVs NaOH (ml)pHV' (ml)d1pH/dVV" (ml)d2pH/V'102.240.500.11.000212.341.500.12.000.1322.442.500.23.000.02432.643.500.224.00-0.05542.864.500.175.000.1653.035.500.276.000.24763.36.500.517.001.97873.817.502.488.001.51986.298.503.999.00-3.6710910.289.500.3210.00-0.12111010.610.500.211.00-0.08121110.811.500.1212.00-0.01131210.9212.500.1113.00-0.03141311.0313.500.0814.00-0.01151411.1114.500.0715.00-0.01161511.1815.500.0616.00-0.03171611.2416.500.0317.000.03181711.2717.500.0618.00-0.01191811.3318.500.0519.00-0.02201911.3819.500.0320.000.02212011.4120.500.0521.00-0.02222111.4621.500.0322.00-0.01232211.4922.500.0223.000.01242311.5123.500.0323.750.9016666667252411.5424.000.480833333324.000.0200347222Masa=0,0997,la equivalent pH=6,8Eg:1000*0,0997/(0,1*1*7,3)136.5753424658

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